Description: Arunachalam, J.; Mohl, C.; Ostapczuk, P.; Emons, H. Fresenius' Jorunal of Analytical Chemistry 352 (1995), 6, 577-581 The recovery of trace elements of ecotoxic importance has been studied on certifed soil and sediment reference samples after pressurized digestions with HNO 3 , HNO 3 + HF and HNO 3 + HCI + HF mixtures, respectively. The acid digests habe been analyzed by ICP-MS. The results indicate that digestion with nitric acid alone is satisfactory for the recovery of As, Cd, Co, Cu and Zn. Cr and Pb showed lower recoveries with HNO 3 alone but addition of HF improved their extraction. With appropriate corrections, ICP-MS can be used for the routine analysis of soils and sediments. These digestion procedures, evaluated based on reference samples, have been used for the trace element characterization of soil samples from the German Environmental Specimen Bank. doi:10.1007/BF00323077
Global identifier:
Doi( "10.1007/BF00323077", )
Types:
Text { text_type: Publication, }
Origin: /Bund/UBA/Umweltprobenbank
Tags: Salpetersäure ? Analytische Chemie ? Spurenelement ? Umweltprobenbank des Bundes ? Bodenprobe ? Bodenuntersuchung ? Sediment ?
License: other-closed
Language: Deutsch
Issued: 1995-01-01
Time ranges: 1995-01-01 - 1995-01-01
doi:10.1007/BF00323077
http://dx.doi.org/10.1007/BF00323077 (Webseite)Accessed 1 times.