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Water content and dry bulk density of pilot core to CON01-603-2, PANGAEA

Water content and dry bulk density of pilot core to CON01-603-2

Wet bulk density (GRAPE) of piston core CON01-604-2 from Posolskoe, PANGAEA

Wet bulk density (GRAPE) of piston core CON01-604-2 from Posolskoe

Raw pollen data from kasten core CON01-603-5 part2 (counts)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Raw pollen data from kasten core CON01-603-5 part1 (%)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Pollen counts from Kasten corer CON01-603-5, CONTINENT Ridge

Pollen counts from Kasten corer CON01-603-5 at CONTINENT Ridge.

Raw pollen data from kasten core CON01-603-5 part2 (%)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Raw pollen data from kasten core CON01-605-5 (Vydrino)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Raw pollen data from piston core CON01-605-3 (Vydrino)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Raw pollen data from kasten core CON01-603-5 part1 (counts)

Sediment slices of 0.5 cm thickness were obtained from gravity core segments and of 1 cm thickness from the Vydrino piston core. Volumetric subsamples of 5 cm3 (10 cm3 in case of the lowermost samples from Continent core) were prepared according to standard procedures, including 7-μm ultrasonic fine-sieving (Cwynar et al., 1979, Fægri et al., 1989 K. Fægri, P.E. Kaland and K. Krzywinski, Textbook of Pollen Analysis (4th edition), John Wiley & Sons, Chichester (1989) 328 pp..Fægri et al., 1989 and PALE Steering Committee, 1994). Two tablets of Lycopodium marker spores were added to each sample for calculating total pollen and spore concentrations (Stockmarr, 1971). Water-free glycerol was used for storage and preparation of microscopic slides. The palynological samples were counted at magnifications of 400–600×, applying 1000× for the identification of difficult pollen types, e.g., including Saxifragaceae, Crassulaceae, and Rosaceae.

Trace element composition of concretions, ICP–MS measurements

In order to get a complete geochemical signature, 14 P-rich concretions, chosen among the different cores, were acid digested (Table 3a and Table 3b). In a clean laboratory, 1.7 to 36 mg of concretions were digested overnight in a concentrated mixture of Suprapur acid (3 ml HCl/2 ml HNO3/1 ml HF) at 90 °C in sealed Teflon beakers. After evaporation to dryness, the residue was dissolved in 2.5 ml of 2% HNO3 Suprapur and diluted to 12 ml with Milli-Q water. During the same procedure, we have also dissolved and analysed, for comparison, a pure vivianite from Anlua, Cameroon (tubular crystals, MRAC collection).

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